dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane

Base Information

• Chemical Name: dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane
• CAS No.: 473543-32-7
• Molecular Formula: C₁₇H₃₁O₂PS
• Molecular Weight: 330.472
• Mol file: 473543-32-7.mol

Synonyms:dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane

Chemical Property of dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane

There total 5 articles about dicyclohexyl-(1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl)-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

dicyclohexyl-(1,1-dioxo-hexahydro-1λ6-thiopyran-4-yl)-phosphane; compound with borane → dicyclohexyl-(1,1-dioxo-hexahydro-1λ6-thiopyran-4-yl)-phosphane (473543-32-7)

Guidance literature:

With morpholine; at 110 ℃; for 2h;

Reference yield:

tetrahydrothiopyran-4-ol (29683-23-6) → dicyclohexyl-(1,1-dioxo-hexahydro-1λ6-thiopyran-4-yl)-phosphane (473543-32-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 98 percent / KIO₄

2: 90 percent / pyridine / CH₂Cl₂

3: 56 percent / tetrahydrofuran / -78 °C

4: 100 percent / morpholine / 2 h / 110 °C

With morpholine; pyridine; potassium metaperiodate; In tetrahydrofuran; dichloromethane;

Reference yield:

Tetrahydrothiopyran-4-one (1072-72-6) → dicyclohexyl-(1,1-dioxo-hexahydro-1λ6-thiopyran-4-yl)-phosphane (473543-32-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 96 percent / NaBH₄

2: 98 percent / KIO₄

3: 90 percent / pyridine / CH₂Cl₂

4: 56 percent / tetrahydrofuran / -78 °C

5: 100 percent / morpholine / 2 h / 110 °C

With morpholine; pyridine; sodium tetrahydroborate; potassium metaperiodate; In tetrahydrofuran; dichloromethane;

upstream raw materials:

tetrahydrothiopyran-4-ol

Tetrahydrothiopyran-4-one

4-hydroxytetrahydro-2H-thiopyrane 1,1-dioxide

trifluoro-methanesulfonic acid 1,1-dioxo-hexahydro-1λ⁶-thiopyran-4-yl ester