(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

Base Information

Chemical Name:(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate
CAS No.:883746-27-8
Molecular Formula:C₂₄H₃₅NO₄
Molecular Weight:401.546
Hs Code.:

Synonyms:(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

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Chemical Property of (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

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Technology Process of (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

There total 3 articles about (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-methyl-2-(1-methylethyl)cyclohexyl (3aR,7aS)-rel-hexahydro-1,2,3-benzothiazole-3(3aH)-carboxylate 2,2-dioxide

: 1863-63-4,21292-26-2,28271-83-2,143502-10-7
ammonium benzoate

: Cyclohex-2-enyl-carbamic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 883746-27-8
(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

: (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1S,2S)-2-(benzoyloxy)cyclohexyl]carbamate

Guidance literature:: 5-methyl-2-(1-methylethyl)cyclohexyl (3aR,7aS)-rel-hexahydro-1,2,3-benzothiazole-3(3aH)-carboxylate 2,2-dioxide; ammonium benzoate; In N,N-dimethyl-formamide; at 45 ℃; for 12h; Inert atmosphere;

With sulfuric acid; water; In tetrahydrofuran; at 20 ℃; for 6h; optical yield given as %de;
DOI:10.1002/ejoc.200900159

Reference yield:

: 883746-44-9
(-)-mentholsulfamoyl chloride

: 883746-27-8
(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / benzene / 1 h / 20 °C

2.1: 30 percent / tetrahydrofuran / 1.5 h / 70 °C

3.1: dimethylformamide / 18 h / 45 °C

3.2: 25 percent / aq. H₂SO₄ / tetrahydrofuran / 6 h / 20 °C

In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1055/s-2006-932450

Reference yield:

: 883746-25-6
N,N-diethyl-N-{[({[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]-oxy}carbonyl)amino]sulfonyl}ethanaminium inner salt

: 883746-27-8
(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl [(1R,2R)-2-(benzoyloxy)cyclohexyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 30 percent / tetrahydrofuran / 1.5 h / 70 °C

2.1: dimethylformamide / 18 h / 45 °C

2.2: 25 percent / aq. H₂SO₄ / tetrahydrofuran / 6 h / 20 °C

In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-932450