1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate

Base Information

• Chemical Name: 1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate
• CAS No.: 1140590-79-9
• Molecular Formula: C₂₅H₃₂N₂O₅
• Molecular Weight: 440.539

Synonyms:1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate

Chemical Property of 1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate

Chemical Property:

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Technology Process of 1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate

There total 1 articles about 1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyloxycarbonylpiperidin-4-one (79099-07-3) + 2-amino-5-benzyloxybenzoic acid methyl ester (116027-17-9) → 1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate (1140590-79-9)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; at 110 ℃; Microwave irradiation;

Reference yield:

1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate (1140590-79-9) + isobutyl chloroformate (543-27-1) → 1,1-Dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl][(2-methyl-propoxy)carbonyl]amino}piperidine-1-carboxylate (1140590-80-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,2-dichloro-ethane; at 80 ℃; Microwave irradiation;

Reference yield:

1,1-dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl]amino}piperidine-1-carboxylate (1140590-79-9) → 1,1-Dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl][(2-methyl-propoxy)carbonyl]amino}piperidine-1-carboxylate (1140590-80-2)

Guidance literature:

With NaOH; DIEA; In ethyl acetate;

upstream raw materials:

N-tert-butyloxycarbonylpiperidin-4-one

2-amino-5-benzyloxybenzoic acid methyl ester

Downstream raw materials:

1,1-Dimethylethyl 4-{[4-(benzyloxy)-2-(methoxycarbonyl)phenyl][(2-methyl-propoxy)carbonyl]amino}piperidine-1-carboxylate

1-(1-acetylpiperidin-4-yl)-3-(3,4-dimethoxybenzyl)-6-hydroxyquinazoline-2,4(1H,3H)-dione

{[1-(1-acetylpiperidin-4-yl)-3-(3,4-dimethoxybenzyl)-2,4-dioxo-1,2,3,4-tetrahydroquinazolin-6-yl]oxy}acetonitrile

{[3-(3,4-dimethoxybenzyl)-1-(1-formylpiperidin-4-yl)-2,4-dioxo-1,2,3,4-tetrahydroquinazolin-6-yl]oxy}acetonitrile

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