(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

Base Information

Chemical Name:(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester
CAS No.:372965-65-6
Molecular Formula:C₂₆H₃₅NO₄
Molecular Weight:425.568
Hs Code.:

Synonyms:(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

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Chemical Property of (S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

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Technology Process of (S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

There total 3 articles about (S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-39-0
benzyl bromide

: 372965-64-5
(S)-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

: 372965-65-6
(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

Guidance literature:: benzyl bromide; (S)-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

In N,N-dimethyl-formamide; at 100 ℃; for 48h;
DOI:10.1002/1522-2675(20010711)84:7<2064::AID-HLCA2064>3.0.CO;2-Y

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 372965-65-6
(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 7.23 g / AcCl / 3 h / 20 °C

2.1: 57 percent / CaO / dimethylformamide / 144 h / 20 °C

3.1: K₂CO₃; Bu₄NI / dimethylformamide / 4 h / 20 °C

3.2: 93 percent / dimethylformamide / 48 h / 100 °C

With tetra-(n-butyl)ammonium iodide; potassium carbonate; acetyl chloride; calcium oxide; In N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(20010711)84:7<2064::AID-HLCA2064>3.0.CO;2-Y

Reference yield:

: 104528-83-8
(S)-(+)-3,4-dimethoxyphenylalanine ethyl ester

: 372965-65-6
(S)-N-benzyl-N-(4-methylpent-3-enyl)-3-(3,4-dimethoxyphenyl)alanine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 57 percent / CaO / dimethylformamide / 144 h / 20 °C

2.1: K₂CO₃; Bu₄NI / dimethylformamide / 4 h / 20 °C

2.2: 93 percent / dimethylformamide / 48 h / 100 °C

With tetra-(n-butyl)ammonium iodide; potassium carbonate; calcium oxide; In N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(20010711)84:7<2064::AID-HLCA2064>3.0.CO;2-Y