Technology Process of C15H14BrClN4O2
There total 5 articles about C15H14BrClN4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bromine; potassium acetate;
In
acetic acid;
at 45 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 3.5 h / 40 °C
1.2: 73 h / 40 - 80 °C
1.3: 1 h / 120 °C / Microwaves
2.1: acetic acid; sodium nitrite / water / 1 h / 80 °C
3.1: sodium dithionite; ammonia / water; acetonitrile / 1.08 h / 80 °C
4.1: 1.5 h / 120 °C
5.1: bromine; potassium acetate / acetic acid / 45 °C
With
sodium dithionite; ammonia; bromine; potassium acetate; acetic acid; N,N-dimethyl-formamide dimethyl acetal; sodium nitrite;
In
water; acetic acid; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; sodium nitrite / water / 1 h / 80 °C
2: sodium dithionite; ammonia / water; acetonitrile / 1.08 h / 80 °C
3: 1.5 h / 120 °C
4: bromine; potassium acetate / acetic acid / 45 °C
With
sodium dithionite; ammonia; bromine; potassium acetate; acetic acid; sodium nitrite;
In
water; acetic acid; acetonitrile;