5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate

Base Information

• Chemical Name: 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate
• CAS No.: 13020-40-1
• Molecular Formula: C₂₀H₁₆N₂O₄
• Molecular Weight: 348.358

Synonyms:5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate

Chemical Property of 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate

Chemical Property:

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Technology Process of 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate

There total 1 articles about 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,2-diamino-benzene (95-54-5) + 2,4-Dihydroxybenzaldehyde (95-01-2) → 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate (13020-40-1)

Guidance literature:

In methanol; at 60 ℃; for 4h;

DOI:10.1080/00958972.2012.699046

Reference yield: 76.0%

diphenyltin(IV) dichloride (1135-99-5) + 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate (13020-40-1) → diphenyl[N,N'-bis(3-hydroxysalicylaldehyde)-1,2-phenylenediiminato]tin(IV) (1621877-43-7)

Guidance literature:

With triethylamine; In ethanol;

DOI:10.1016/j.jorganchem.2014.07.002

Reference yield:

chlorophosphoric acid diphenyl ester (2524-64-3) + 5,5'-dihydroxy-2,2'-[o-phenylenebis(nitrilomethylene)]diphenol ethanol solvate (13020-40-1) → N,N′-bis( 2-hydroxy-4 (diphenyl phosphate)sulfinyl)-1,2-phenylenediamine

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 30 ℃; for 6h; Inert atmosphere;

upstream raw materials:

1,2-diamino-benzene

2,4-Dihydroxybenzaldehyde

Downstream raw materials:

diphenyl[N,N'-bis(3-hydroxysalicylaldehyde)-1,2-phenylenediiminato]tin(IV)

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