methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

Base Information

Chemical Name:methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside
CAS No.:84730-84-7
Molecular Formula:C₂₉H₃₈O₁₇S
Molecular Weight:690.677
Hs Code.:

Synonyms:methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

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Technology Process of methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

There total 1 articles about methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 124-63-0
methanesulfonyl chloride

: 16790-35-5
methyl 4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 84730-84-7
methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

Guidance literature:: In pyridine; at 0 ℃;
DOI:10.1016/0008-6215(83)88267-6

Reference yield: 68.0%

: 532-32-1
sodium benzoate

: 84730-84-7
methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

: 84730-87-0
methyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-allopyranoside

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 25h;
DOI:10.1016/0008-6215(83)88267-6

Reference yield:

: 84730-84-7
methyl 2',3',4',6'-tetra-O-acetyl-4,6-O-benzylidene-3-O-(methylsulfonyl)-β-sophoroside

: 84730-88-1
methyl 4,6-O-benzylidene-2-O-β-D-glucopyranosyl-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / dimethylformamide / 25 h / 90 °C

2: 89 percent / sodium methoxide / methanol / 1 h / Ambient temperature

With sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(83)88267-6