0Aka1qwt6Q

Base Information

Chemical Name:0Aka1qwt6Q
CAS No.:359844-37-4
Molecular Formula:C₉H₁₁BrO₃
Molecular Weight:247.089
Hs Code.:
UNII:0AKA1QWT6Q

Synonyms:0AKA1QWT6Q;UNII-0AKA1QWT6Q;4-Bromo-2-hydroxy-5-methoxybenzeneethanol;Benzeneethanol, 4-bromo-2-hydroxy-5-methoxy-;2-(4-bromo-2-hydroxy-5-methoxyphenyl)-ethanol;359844-37-4

Suppliers and Price of 0Aka1qwt6Q

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 0Aka1qwt6Q

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:245.98916
Heavy Atom Count:13
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)CCO)O)Br

Technology Process of 0Aka1qwt6Q

There total 5 articles about 0Aka1qwt6Q which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[4-bromo-2-(tert-butyl-dimethyl-silanyloxy)-5-methoxy-phenyl]-ethanol

: 359844-37-4
3-bromo-6-(2'-hydroxy)ethyl-4-methoxyphenol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/jo000696e

Reference yield:

: 17332-12-6
3-bromo-4-methoxy-phenol

: 359844-37-4
3-bromo-6-(2'-hydroxy)ethyl-4-methoxyphenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-diethylaniline / 4 h / Heating

2.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

3.1: OsO₄; NaIO₄ / diethyl ether; acetone; H₂O / 8 h

3.2: sodium borohydride / methanol / 0.5 h / 0 °C

4.1: tetra-n-butylammonium fluoride / CH₂Cl₂; tetrahydrofuran / 1 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; triethylamine; N,N-diethylaniline; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; 2.1: Claisen rearrangement;
DOI:10.1021/jo000696e

Reference yield:

: 74097-29-3
2-allyl-5-bromo-4-methoxyphenol

: 359844-37-4
3-bromo-6-(2'-hydroxy)ethyl-4-methoxyphenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

2.1: OsO₄; NaIO₄ / diethyl ether; acetone; H₂O / 8 h

2.2: sodium borohydride / methanol / 0.5 h / 0 °C

3.1: tetra-n-butylammonium fluoride / CH₂Cl₂; tetrahydrofuran / 1 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone;
DOI:10.1021/jo000696e