ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

Base Information

Chemical Name:ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate
CAS No.:89358-88-3
Molecular Formula:C₂₁H₃₆O₆
Molecular Weight:384.513
Hs Code.:

Synonyms:ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

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Technology Process of ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

There total 2 articles about ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65391-47-1
(E)-ethyl 3-((4R,5S)-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)2,2-dimethyl-1,3-dioxolan-4-yl)acrylate

: 931-50-0
cyclohexylmagnesium bromide

: 89358-88-3
ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

: 89358-87-2
ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-manno-heptonate

Guidance literature:: With copper(l) iodide; In diethyl ether; at -70 ℃; for 5h;
DOI:10.1039/P19830002629

Reference yield:

: 13039-93-5
2,2:4,5-di-O-isopropylidene-D-arabinose

: 89358-88-3
ethyl 3C-cyclohexyl-2,3-dideoxy-4,5:6,7-di-O-isopropylidene-D-gluco-heptonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) benzene, 20 deg C, 1 h, 2.) 20 - 25 deg C, 5 min

2: cuprous iodide / diethyl ether / 5 h / -70 °C

With copper(l) iodide; sodium hydride; In diethyl ether;
DOI:10.1039/P19830002629