(((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene

Base Information

• Chemical Name: (((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene
• CAS No.: 80595-07-9
• Molecular Formula: C₂₂H₂₆O₂
• Molecular Weight: 322.447
• Mol file: 80595-07-9.mol

Synonyms:(((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene

Chemical Property of (((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene

There total 1 articles about (((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + 1,1-bis(hydroxymethyl)cyclohex-3-ene disodium → (((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene (80595-07-9)

Guidance literature:

In benzene; for 4h; Heating;

DOI:10.1021/jo00346a015

Reference yield:

(((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene (80595-07-9) + acetyl chloride (75-36-5) → 1,1-bis(acetoxymethyl)cyclohex-3-ene (27025-19-0) + benzyl chloride (100-44-7)

Guidance literature:

With trans benzyl(chloro)bis(triphenylphosphine)palladium(II); tributyltin chloride; at 63 ℃; for 48h;

DOI:10.1021/jo00346a015

Reference yield:

(((cyclohex-3-ene-1,1-diylbis(methylene))bis(oxy))bis(methylene))dibenzene (80595-07-9) → C22H26O6 (1430117-91-1)

Guidance literature:

With potassium permanganate; tetrabutylammomium bromide; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/ol400755x

upstream raw materials:

benzyl bromide

Downstream raw materials:

1,1-bis(acetoxymethyl)cyclohex-3-ene

benzyl chloride

C₂₂H₂₆O₆

dimethyl 3,3-bis((benzyloxy)methyl)hexanedioate