N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

Base Information

Chemical Name:N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea
CAS No.:198271-89-5
Molecular Formula:C₃₉H₃₆N₂O₁₁S
Molecular Weight:740.788
Hs Code.:

Synonyms:N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

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Chemical Property of N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

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Technology Process of N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

There total 4 articles about N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 459-73-4
GlyOEt*HCl

: 198271-81-7
2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl isothiocyanate

: 198271-89-5
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

Guidance literature:: With Etifelmin; In toluene; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(97)10070-9

Reference yield:

: 138811-45-7
1,2,3,5,6-penta-O-benzoyl-D-galactofuranose

: 198271-89-5
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: Me₃SiBr / CH₂Cl₂ / 24 h / Ambient temperature

2: acetone / 2 h / Ambient temperature

3: 86 percent / EDPA / toluene / 3 h / Ambient temperature

With trimethylsilyl bromide; Etifelmin; In dichloromethane; acetone; toluene;
DOI:10.1016/S0040-4020(97)10070-9

Reference yield:

: 153923-40-1
2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl bromide

: 198271-89-5
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-N'-carboxyethylmethylene thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 2 h / Ambient temperature

2: 86 percent / EDPA / toluene / 3 h / Ambient temperature

With Etifelmin; In acetone; toluene;
DOI:10.1016/S0040-4020(97)10070-9