tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside

Base Information

• Chemical Name: tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside
• CAS No.: 1198214-95-7
• Molecular Formula: C₄₅H₅₃NO₁₁Si
• Molecular Weight: 812.001

Synonyms:tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside

Chemical Property of tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside

There total 1 articles about tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(fluorenylmethoxy)carbonyl chloride (28920-43-6) + tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleoyl-3-O-levulinyl-β-D-glucopyranoside (385422-24-2) → tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside (1198214-95-7)

Guidance literature:

With dmap; In pyridine; at 0 ℃;

DOI:10.1002/ejoc.200900627

Reference yield:

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside (1198214-95-7) → tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranoside (1198214-79-7)

Guidance literature:

With hydrazinium monoacetate; In methanol; dichloromethane; at 20 ℃; for 16h;

DOI:10.1002/ejoc.200900627

Reference yield:

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-3-O-levulenoyl-β-D-glucopyranoside (1198214-95-7) → tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleoyl-3-O-levulinyl-β-D-glucopyranoside (385422-24-2)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1002/ejoc.200900627

upstream raw materials:

(fluorenylmethoxy)carbonyl chloride

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleoyl-3-O-levulinyl-β-D-glucopyranoside

Downstream raw materials:

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranoside

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleimido-4-O-levulenoyl-β-D-glucopyranoside

tert-butyldimethylsilyl 6-O-benzyl-2-deoxy-2-dimethylmaleoyl-3-O-levulinyl-β-D-glucopyranoside

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