4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

Base Information

Chemical Name:4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine
CAS No.:443642-58-8
Molecular Formula:C₂₇H₂₂Cl₅N₃O₄
Molecular Weight:629.754
Hs Code.:

Synonyms:4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

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Chemical Property of 4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

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Technology Process of 4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

There total 6 articles about 4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 443643-38-7
3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-1-O-methyl-α-D-ribofuranose

: 4-chloro-1H-pyrrolo[2,3-d]pyrimidine sodium salt

: 443642-58-8
4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: 3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-1-O-methyl-α-D-ribofuranose; With hydrogen bromide; In dichloromethane; acetic acid; at -10 - 0 ℃; for 4h;

4-chloro-1H-pyrrolo[2,3-d]pyrimidine sodium salt; In acetonitrile; at 20 ℃; for 24h;

Reference yield:

: 443643-38-7
3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-1-O-methyl-α-D-ribofuranose

: 443642-59-9
sodium salt of 4-chloro-1H-pyrrolo[2,3-d]pyrimidine

: 443642-58-8
4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: With hydrogen bromide; SiO₂; In dichloromethane; water; acetic acid; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 443642-30-6
3,5-bis-O-(2,4-dichlorophenylmethyl)-1-O-methyl-α-D-erythro-pentafuranos-2-ulose

: 443642-58-8
4-chloro-7-[3,5-bis-O-(2,4-dichlorophenylmethyl)-2-C-vinyl-β-D-ribofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride / SiO₂ / tetrahydrofuran; ethyl acetate

2: hydrogen bromide / SiO₂ / dichloromethane; water; acetic acid; ethyl acetate; toluene; acetonitrile

With ammonium chloride; hydrogen bromide; SiO₂; In tetrahydrofuran; dichloromethane; water; acetic acid; ethyl acetate; toluene; acetonitrile;