1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

Base Information

Chemical Name:1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester
CAS No.:1259438-01-1
Molecular Formula:C₁₈H₁₅FN₂O₂
Molecular Weight:310.328
Hs Code.:

Synonyms:1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

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Chemical Property of 1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

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Technology Process of 1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

There total 4 articles about 1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1082469-90-6
(Z)-3-(4-fluorophenylamino)-but-2-enoic acid methylester

: 100-47-0
benzonitrile

: 1259438-01-1
1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

Guidance literature:: With copper diacetate; at 120 ℃; regioselective reaction;
DOI:10.1002/anie.201002389

Reference yield: 64.0%

: C₁₁H₁₂FNO₂

: 100-47-0
benzonitrile

: 1259438-01-1
1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

Guidance literature:: With copper diacetate; at 120 ℃; for 1h; Microwave irradiation;
DOI:10.1016/j.bmcl.2013.09.039

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 1259438-01-1
1-(4-fluorophenyl)-5-methyl-3-phenyl-1H-pyrazole-4-carboxylic acid methylester

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) bromide / methanol / 18 h / 20 °C / Molecular sieve

2: copper diacetate / 1 h / 120 °C / Microwave irradiation

With indium(III) bromide; copper diacetate; In methanol;
DOI:10.1016/j.bmcl.2013.09.039