O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Base Information

Chemical Name:O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol
CAS No.:640279-64-7
Molecular Formula:C₃₁H₄₃NO₅
Molecular Weight:509.686
Hs Code.:

Synonyms:O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

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Technology Process of O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

There total 4 articles about O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6125-24-2
2-Phenylnitroethane

: 640279-64-7
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: Multi-step reaction with 3 steps

1: activated Al₂O₃ / 24 h / -20 °C

2: H₂ / Raney-Ni / methanol / 16 h / 20 °C

3: 185 mg / aq. NaHCO₃ / ethyl acetate / 2 h / 20 °C

With aluminum oxide; hydrogen; sodium hydrogencarbonate; nickel; In methanol; ethyl acetate;
DOI:10.1021/jo0358269

Reference yield:

: 84312-20-9
(1R,3R,4S)-8-phenylmenthyl glyoxylate

: 640279-64-7
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: Multi-step reaction with 3 steps

1: activated Al₂O₃ / 24 h / -20 °C

2: H₂ / Raney-Ni / methanol / 16 h / 20 °C

3: 185 mg / aq. NaHCO₃ / ethyl acetate / 2 h / 20 °C

With aluminum oxide; hydrogen; sodium hydrogencarbonate; nickel; In methanol; ethyl acetate;
DOI:10.1021/jo0358269

Reference yield:

: 640279-63-6
O-[(2S)-hydroxy-(3R)-3-nitro-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

: 640279-64-7
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney-Ni / methanol / 16 h / 20 °C

2: 185 mg / aq. NaHCO₃ / ethyl acetate / 2 h / 20 °C

With hydrogen; sodium hydrogencarbonate; nickel; In methanol; ethyl acetate;
DOI:10.1021/jo0358269