3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-, 3-(1,1-dimethylethyl) 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester, (4R,5S)-

Base Information

Chemical Name:3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-, 3-(1,1-dimethylethyl) 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester, (4R,5S)-
CAS No.:685508-06-9
Molecular Formula:C34H47NO5
Molecular Weight:549.751
Hs Code.:

3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-,
3-(1,1-dimethylethyl)
5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester,
(4R,5S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-, 3-(1,1-dimethylethyl) 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester, (4R,5S)-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-, 3-(1,1-dimethylethyl) 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester, (4R,5S)-

There total 6 articles about 3,5-Oxazolidinedicarboxylic acid, 2,2-dimethyl-4-(phenylmethyl)-, 3-(1,1-dimethylethyl) 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] ester, (4R,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 77-76-9
2,2-dimethoxy-propane

: 640279-64-7
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

: 685508-06-9
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-2,3-isopropylidene-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 50 ℃; for 5h;
DOI:10.1021/jo0358269

Reference yield:

: 6125-24-2
2-Phenylnitroethane

: 685508-06-9
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-2,3-isopropylidene-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: Multi-step reaction with 4 steps

1: activated Al₂O₃ / 24 h / -20 °C

2: H₂ / Raney-Ni / methanol / 16 h / 20 °C

3: 185 mg / aq. NaHCO₃ / ethyl acetate / 2 h / 20 °C

4: 87 percent / TsOH / toluene / 5 h / 50 °C

With aluminum oxide; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; nickel; In methanol; ethyl acetate; toluene;
DOI:10.1021/jo0358269

Reference yield:

: 84312-20-9
(1R,3R,4S)-8-phenylmenthyl glyoxylate

: 685508-06-9
O-[(3R)-tert-butoxycarbonylamino-(2S)-hydroxy-2,3-isopropylidene-4-phenylbutanoyl]-(1'R,2'S,5'R)-8'-phenylmenthol

Guidance literature:: Multi-step reaction with 4 steps

1: activated Al₂O₃ / 24 h / -20 °C

2: H₂ / Raney-Ni / methanol / 16 h / 20 °C

3: 185 mg / aq. NaHCO₃ / ethyl acetate / 2 h / 20 °C

4: 87 percent / TsOH / toluene / 5 h / 50 °C

With aluminum oxide; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; nickel; In methanol; ethyl acetate; toluene;
DOI:10.1021/jo0358269