methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

Base Information

Chemical Name:methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate
CAS No.:1369957-48-1
Molecular Formula:C₁₈H₁₈ClNO₄S
Molecular Weight:379.864
Hs Code.:

Synonyms:methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

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Chemical Property of methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

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Technology Process of methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

There total 4 articles about methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369957-47-0
4-chloro-N-{4-[(2-oxotetrahydrofuran-3-yl)sulfanyl]phenyl}benzamide

: 74-88-4
methyl iodide

: 1369957-48-1
methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

Guidance literature:: 4-chloro-N-{4-[(2-oxotetrahydrofuran-3-yl)sulfanyl]phenyl}benzamide; With water; sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; With 18-crown-6 ether; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1369957-48-1
methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: sodium hydroxide; water / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 20 °C

With water; hydrogen; triethylamine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1369800-50-9
α-[(4-nitrophenyl)thio]-γ-butyrolactone

: 1369957-48-1
methyl 2-[(4-{[(4-chlorophenyl)carbonyl]amino}phenyl)sulfanyl]-4-hydroxybutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h / 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide; water / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 20 °C

With water; hydrogen; triethylamine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;