N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane

Base Information

• Chemical Name: N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane
• CAS No.: 84944-17-2
• Molecular Formula: C₃₂H₄₁N₃O₆S₂
• Molecular Weight: 627.826

Synonyms:N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane

Chemical Property of N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane

Chemical Property:

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Technology Process of N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane

There total 1 articles about N²,N⁹-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

N,N'-ditosyl-1,6-diaminohexane (69762-22-7) + 5'-Deoxy-2',5'-dichloro-3,4'-O-isopropylidene-6-methylpyridoxine Hydrochloride (83492-42-6) → N2,N9-Di-p-tosyl-15-hydroxy-16-hydroxymethyl-15,16'-O-isopropylidene-12-methyl-2,9-diaza<10>(2,5)pyridinophane (84944-17-2)

Guidance literature:

In N,N-dimethyl-formamide; at 60 ℃; for 2.5h;

DOI:10.1021/jo00156a027

upstream raw materials:

N,N'-ditosyl-1,6-diaminohexane

5'-Deoxy-2',5'-dichloro-3,4'-O-isopropylidene-6-methylpyridoxine Hydrochloride

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