(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

Base Information

Chemical Name:(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex
CAS No.:946490-04-6
Molecular Formula:C₂₄H₂₀N₂O₄Ru
Molecular Weight:501.504
Hs Code.:

Synonyms:(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

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Chemical Property of (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

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Technology Process of (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

There total 1 articles about (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 88288-78-2
1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one

: 946490-04-6
(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

Guidance literature:: With oxygen; In toluene; Schlenk technique; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.1c00654

Reference yield: 84.0%

: 946490-04-6
(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

: 109-63-7
boron trifluoride diethyl etherate

: C₂₅H₂₅N₂O₃Ru⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201412207

Reference yield: 65.0%

: 946490-04-6
(1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex

: 603-35-0
triphenylphosphine

: (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one) triphenylphosphine dicarbonyl ruthenium complex

Guidance literature:: With oxygen; In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.1c00654