[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Base Information

Chemical Name:[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine
CAS No.:122488-45-3
Molecular Formula:C₁₅H₁₄ClF₃N₆
Molecular Weight:370.765
Hs Code.:

Synonyms:[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

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Chemical Property of [9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

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Technology Process of [9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

There total 6 articles about [9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 122488-44-2
[9-(4-Chloro-3-nitro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

: 122488-45-3
[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 1h; under 1520 - 2280 Torr;
DOI:10.1021/jm00128a016

Reference yield:

: 55912-20-4
4-chloro-3-nitrobenzyl alcohol

: 122488-45-3
[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: PBr₃ / toluene / 0.17 h / 100 °C

2: 54 percent

3: 75 percent / ethanol

4: 79 percent / H₂ / 5percent Pd/C / acetic acid / 1 h / 1520 - 2280 Torr

With hydrogen; phosphorus tribromide; palladium on activated charcoal; In ethanol; acetic acid; toluene;
DOI:10.1021/jm00128a016

Reference yield:

: 1998-63-6
6-chloro-2-(trifluoromethyl)-9H-purine

: 122488-45-3
[9-(3-Amino-4-chloro-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent

2: 75 percent / ethanol

3: 79 percent / H₂ / 5percent Pd/C / acetic acid / 1 h / 1520 - 2280 Torr

With hydrogen; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00128a016