(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

Base Information

Chemical Name:(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride
CAS No.:1028295-36-4
Molecular Formula:C₁₉H₂₇F₂IO₂
Molecular Weight:452.323
Hs Code.:

Synonyms:(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

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Chemical Property of (E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

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Technology Process of (E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

There total 2 articles about (E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2777-66-4
methyl 10-undecynoate

: 371-11-9
4-(difluoroiodo)toluene

: 1028295-36-4
(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

Guidance literature:: With triethylamine pentahydrogen fluoride salt; In dichloromethane; for 1h;
DOI:10.1039/a801273c

Reference yield:

: 624-31-7
4-tolyl iodide

: 1028295-36-4
(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N*5HF / 20 °C / Electrochemical reaction

2: Et₃N*5HF / CH₂Cl₂ / 8 h / 0 °C

With triethylamine pentahydrogen fluoride salt; In dichloromethane;
DOI:10.1039/b101836l

Reference yield: 59.0%

: 693-02-7
hex-1-yne

: 1028295-36-4
(E)-(2-fluoro-10-methoxycarbonyl-1-decenyl)(4-methylphenyl)iodonium fluoride

: 180071-98-1
1-(p-tolyl)-1-hexyne

: methyl (E)-10-fluoro-10-heptadecen-12-ynoate

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0040-4020(01)00683-4