(2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

Base Information

Chemical Name:(2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide
CAS No.:123506-05-8
Molecular Formula:C₄₉H₆₄BrNO₁₁
Molecular Weight:922.951
Hs Code.:

(2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

Synonyms:(2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

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Chemical Property of (2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

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Technology Process of (2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

There total 8 articles about (2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123505-99-7
(2S,3R,4S,4aS,5S,6S,8aS)-4,5-Bis-benzyloxy-2-isopropenyl-6-(4-methoxy-benzyloxy)-3-methoxymethoxymethyl-6-methyl-hexahydro-pyrano[2,3-b]pyran

: 123506-05-8
(2S,3R,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((3S,4R,5R)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 9-BBN, 2.) Na₂O₂ / 1.) THF

2: PCC, Celite, Fluorisil, NaOAC / CH₂Cl₂

3: tetrahydrofuran / -90 °C

4: 1.) NaH, 2.) n-Bu₄NI / 1.) DMF

5: 86 percent / NBS, NaHCO₃ / acetonitrile

6: 1.) Swern's oxid. / 2.) CH₂Cl₂

With N-Bromosuccinimide; 9-borabicyclo[3.3.1]nonane dimer; sodium peroxide; Florisil; Celite; Swern's oxid; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo00284a030

Reference yield:

: 123506-00-3
2-[(2R,3R,4S,4aS,5S,6S,8aS)-4,5-Bis-benzyloxy-6-(4-methoxy-benzyloxy)-3-methoxymethoxymethyl-6-methyl-hexahydro-pyrano[2,3-b]pyran-2-yl]-propan-1-ol

: 123506-05-8
(2S,3R,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((3S,4R,5R)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 5 steps

1: PCC, Celite, Fluorisil, NaOAC / CH₂Cl₂

2: tetrahydrofuran / -90 °C

3: 1.) NaH, 2.) n-Bu₄NI / 1.) DMF

4: 86 percent / NBS, NaHCO₃ / acetonitrile

5: 1.) Swern's oxid. / 2.) CH₂Cl₂

With N-Bromosuccinimide; Florisil; Celite; Swern's oxid; sodium acetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo00284a030

Reference yield:

: 123506-01-4
2-[(2S,3R,4S,4aS,5S,6S,8aS)-4,5-Bis-benzyloxy-6-(4-methoxy-benzyloxy)-3-methoxymethoxymethyl-6-methyl-hexahydro-pyrano[2,3-b]pyran-2-yl]-propionaldehyde

: 123506-05-8
(2S,3R,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((3S,4R,5R)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / -90 °C

2: 1.) NaH, 2.) n-Bu₄NI / 1.) DMF

3: 86 percent / NBS, NaHCO₃ / acetonitrile

4: 1.) Swern's oxid. / 2.) CH₂Cl₂

With N-Bromosuccinimide; Swern's oxid; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00284a030