(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Base Information

Chemical Name:(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide
CAS No.:129163-46-8
Molecular Formula:C₄₉H₆₂BrNO₁₁
Molecular Weight:920.935
Hs Code.:

(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Synonyms:

Suppliers and Price of (2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

There total 3 articles about (2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 123506-05-8
(2S,3S,4S)-3-Benzyloxy-2-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-hydroxy-4-(4-methoxy-benzyloxy)-4-methyl-pentanoic acid methoxy-methyl-amide

: 129163-46-8,129214-42-2
(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Guidance literature:: With molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)97592-1

Reference yield:

: 123506-02-5
(2S,3R,4S,4aS,5R,6S,8aS)-4,5-Bis-benzyloxy-2-((1S,2R)-2-benzyloxy-1,3-dimethyl-but-3-enyl)-6-(4-methoxy-benzyloxy)-3-methoxymethoxymethyl-6-methyl-hexahydro-pyrano[2,3-b]pyran

: 129163-46-8,129214-42-2
(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / acetonitrile

2: CH₂Cl₂ / Ambient temperature

3: 82 percent / molecular sieves, 2,3-dichloro-5,6-dicyano-1,2-benzoquinone / CH₂Cl₂ / 0.25 h / Ambient temperature

With N-Bromosuccinimide; molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)97592-1

Reference yield:

: 123506-04-7
(3S,4R,5S)-4-Benzyloxy-3-[(1S,2R)-1-benzyloxy-2-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-3-methoxymethoxy-propyl]-5-(4-methoxy-benzyloxy)-5-methyl-tetrahydro-pyran-2-one

: 129163-46-8,129214-42-2
(2S,3S,4R)-3-Benzyloxy-4-((2R,3S,4R,5S)-4-benzyloxy-5-bromomethyl-3,5-dimethyl-tetrahydro-furan-2-yl)-2-{(S)-benzyloxy-[(S)-2-(4-methoxy-phenyl)-4-methyl-[1,3]dioxolan-4-yl]-methyl}-5-methoxymethoxy-pentanoic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / Ambient temperature

2: 82 percent / molecular sieves, 2,3-dichloro-5,6-dicyano-1,2-benzoquinone / CH₂Cl₂ / 0.25 h / Ambient temperature

With molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1016/S0040-4020(01)97592-1