(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

Base Information

Chemical Name:(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone
CAS No.:618888-66-7
Molecular Formula:C₁₇H₂₀O₇
Molecular Weight:336.342
Hs Code.:

Synonyms:(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

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Technology Process of (1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

There total 1 articles about (1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 183474-89-7
(1S,3S,4R,5R)-3-allyl-1-hydroxy-7-oxo-6-oxabicyclo[3.2.1]oct-4-yl benzoate

: 618888-66-7
(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In acetone; tert-butyl alcohol; at 20 ℃; for 20h;
DOI:10.1039/b301731a

Reference yield: 83.0%

: 67-56-1
methanol

: 618888-66-7
(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

: 618888-69-0
methyl (1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-1,3,4-trihydroxycyclohexane-1-carboxylate

Guidance literature:: With sodium methylate; at 20 ℃; for 6h;
DOI:10.1039/b301731a

Reference yield:

: 618888-66-7
(1S,3R,4R,5S)-5-(2',3'-dihydroxypropyl)-4-benzoyl-1-hydroxycyclohexane-1,3-carbolactone

: (1S,3S,4R,5R)-3-(2,3-Dihydroxy-propyl)-1,4,5-trihydroxy-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NaOMe / 6 h / 20 °C

2: 100 percent / aq. NaOH / 20 °C / pH 12

With sodium hydroxide; sodium methylate;
DOI:10.1039/b301731a