5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

Base Information

Chemical Name:5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione
CAS No.:1384978-85-1
Molecular Formula:C₁₃H₁₃N₅OS
Molecular Weight:287.345
Hs Code.:

Synonyms:5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

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Chemical Property of 5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

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Technology Process of 5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

There total 3 articles about 5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 506-68-3
bromocyane

: 1345840-60-9
6-methyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carbohydrazide

: 1384978-85-1
5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

Guidance literature:: With sodium hydrogencarbonate; In ethanol;
DOI:10.1016/j.cclet.2012.05.004

Reference yield:

: 100-52-7
benzaldehyde

: 1384978-85-1
5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

Guidance literature:: Multi-step reaction with 3 steps

1: calcium chloride / ethanol / Reflux

2: sulfuric acid; hydrazine hydrate / ethanol

3: sodium hydrogencarbonate / ethanol

With sulfuric acid; sodium hydrogencarbonate; hydrazine hydrate; calcium chloride; In ethanol;
DOI:10.1016/j.cclet.2012.05.004

Reference yield:

: 123043-88-9,33458-26-3
5-ethoxycarbonyl-4-phenyl-6-methyl-3,4-dihydropyrimidine-2(1H)-thione

: 1384978-85-1
5-(5-amino-1,3,4-oxadiazol-2-yl)-6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; hydrazine hydrate / ethanol

2: sodium hydrogencarbonate / ethanol

With sulfuric acid; sodium hydrogencarbonate; hydrazine hydrate; In ethanol;
DOI:10.1016/j.cclet.2012.05.004