7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

Base Information

Chemical Name:7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine
CAS No.:154379-13-2
Molecular Formula:C₁₃H₁₀BrN₃O₂
Molecular Weight:320.145
Hs Code.:

Synonyms:7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

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Technology Process of 7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

There total 1 articles about 7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 539-74-2
Ethyl 3-bromopropionate

: 56741-95-8
bropirimine

: 154379-13-2
7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

Guidance literature:: With potassium carbonate; In isopropyl alcohol; at 75 ℃; for 18h;
DOI:10.1002/jhet.5570300517

Reference yield: 63.0%

: 105-36-2
ethyl bromoacetate

: 154379-13-2
7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

: 154379-19-8
7-bromo-1-ethoxycarbonylmethyl-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

Guidance literature:: With potassium carbonate; In 1,4-dioxane; at 90 - 100 ℃; for 24h;
DOI:10.1002/jhet.5570300517

Reference yield: 41.0%

: 5407-04-5
3-(dimethylamino)propyl chloride hydrochloride

: 154379-13-2
7-bromo-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

: 7-bromo-1-(3-dimethylaminopropyl)-4,6-dioxo-8-phenyl-2,3,4,6-tetrahydro-1H-pyrimido<1,2-a>pyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; isopropyl alcohol; at 75 - 85 ℃; for 16h;
DOI:10.1002/jhet.5570300517