Technology Process of C13H18O
There total 7 articles about C13H18O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-methyl-4-(1-methylcyclopent-3-enyl)benzene;
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 0 ℃;
for 4h;
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
DOI:10.1080/00397911.2010.494812
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C
2.1: diethylzinc / hexane; dichloromethane / 12 h / -20 °C / Inert atmosphere
3.1: pyridine; carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / 20 °C
4.1: 2,2'-azobis(isobutyronitrile) / benzene / 12 h / Inert atmosphere; Reflux
5.1: Grubbs catalyst first generation / benzene / 3 h / Reflux
6.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C
6.2: 0 - 20 °C
With
pyridine; Grubbs catalyst first generation; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); carbon tetrabromide; dimethylsulfide borane complex; diethylzinc; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; benzene;
DOI:10.1080/00397911.2010.494812
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,2'-azobis(isobutyronitrile) / benzene / 12 h / Inert atmosphere; Reflux
2.1: Grubbs catalyst first generation / benzene / 3 h / Reflux
3.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C
3.2: 0 - 20 °C
With
Grubbs catalyst first generation; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex;
In
tetrahydrofuran; benzene;
DOI:10.1080/00397911.2010.494812
