N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

Base Information

Chemical Name:N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide
CAS No.:433710-00-0
Molecular Formula:C₂₁H₁₉N₅O₂
Molecular Weight:373.414
Hs Code.:

Synonyms:N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

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Technology Process of N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

There total 6 articles about N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 433709-98-9
N-benzyl-2-(8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

: 74-88-4
methyl iodide

: 433710-00-0
N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 1h;
DOI:10.1016/j.bmcl.2009.01.093

Reference yield:

: 1149758-76-8
4-((2-(benzylamino)-2-oxoethyl)amino)-2-phenylpyrimidine-5-carboxylic acid

: 433710-00-0
N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Cooling with ice

With diphenyl phosphoryl azide; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/bkcs.10979

Reference yield:

: 226954-91-2
2-(5-ethoxycarbonyl-2-phenylpyrimidine-4-ylamino)acetic acid

: 433710-00-0
N-benzyl-2-(7-methyl-8-oxo-2-phenyl-7,8-dihydro-9H-purin-9-yl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 1 h / 20 °C

2: sodium hydroxide / ethanol; water / 2 h / 80 °C

3: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Cooling with ice

With diphenyl phosphoryl azide; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/bkcs.10979