{(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆

Base Information

• Chemical Name: {(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆
• CAS No.: 134388-31-1
• Molecular Formula: C₃₃H₃₉CuN₆P*F₆P
• Molecular Weight: 759.197

Synonyms:{(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆

Chemical Property of {(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆

Chemical Property:

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Technology Process of {(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆

There total 4 articles about {(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu(P(C₆H₅)3)}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

{((C3H2NNCH3(CH3))3Cu)2O2}(2+) + triphenylphosphine (603-35-0) → {(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}(1+)*PF6(1-)={(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}PF6 (134388-31-1) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

In dichloromethane; slow addn. of PPh3 to the peroxo-dicopper(II) complex; elem. anal.;

DOI:10.1021/ja00012a054

Reference yield: 67.0%

{(C3H2NNCH3(CH3))3Cu}(1+)*PF6(1-)={(C3H2NNCH3(CH3))3Cu}PF6 (134388-28-6) → {(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}(1+)*PF6(1-)={(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}PF6 (134388-31-1)

Guidance literature:

With O₂; P(C₆H₅)3; In dichloromethane; byproducts: OP(C6H5)3; under Ar; through a soln. of the starting complex in CH2Cl2 is bubbled O2 at -90°C to obtain the dioxygen-complex, PPh3 is added, stirred for 3 h, warmed to room temp., stirred overnight; filtd., the filtrate is evapd., the solid is washed, recrystd., elem. anal.;

DOI:10.1021/ja00077a027

Reference yield:

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) → {(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}(1+)*PF6(1-)={(C3H2NNCH3(CH3))3Cu(P(C6H5)3)}PF6 (134388-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; nitromethane

2: O₂; P(C₆H₅)3 / dichloromethane

With O₂; P(C₆H₅)3; In methanol; nitromethane; dichloromethane;

DOI:10.1021/ja00077a027

upstream raw materials:

triphenylphosphine

{(C₃H₂NNCH₃(CH₃))3Cu}⁽¹⁺⁾*PF₆^(1-)={(C₃H₂NNCH₃(CH₃))3Cu}PF₆

tetrakis(actonitrile)copper(I) hexafluorophosphate

1,2-dimethyl-1H-imidazole

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