N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

Base Information

Chemical Name:N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane
CAS No.:198271-82-8
Molecular Formula:C₃₇H₃₃NO₁₀S
Molecular Weight:683.736
Hs Code.:

Synonyms:N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

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Chemical Property of N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

Chemical Property:

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Technology Process of N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

There total 4 articles about N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 64-17-5
ethanol

: 198271-81-7
2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl isothiocyanate

: 198271-82-8
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

Guidance literature:: at 60 ℃;
DOI:10.1016/S0040-4020(97)10070-9

Reference yield:

: 138811-45-7
1,2,3,5,6-penta-O-benzoyl-D-galactofuranose

: 198271-82-8
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride; HCl / 20 °C

2: 89 percent / acetone / 2 h / 20 °C

3: 90 percent

With hydrogenchloride; acetyl chloride; In acetone; 1: Chlorination / 2: Substitution / 3: Addition;
DOI:10.1016/S0008-6215(97)00242-5

Reference yield:

: 201738-27-4
C₃₄H₂₇ClO₉

: 198271-82-8
N-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-O-ethyl thiourethane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetone / 2 h / 20 °C

2: 90 percent

In acetone; 1: Substitution / 2: Addition;
DOI:10.1016/S0008-6215(97)00242-5