PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

Base Information

Chemical Name:PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]
CAS No.:18460-53-2
Molecular Formula:AlCl₄*Cl₄P
Molecular Weight:341.579
Hs Code.:

PCl<sub>4</sub><sup>(1+)</sup>*AlCl<sub>4</sub><sup>(1-)</sup>=PCl<sub>4</sub>[AlCl<sub>4</sub>]

Synonyms:PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

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Chemical Property of PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

Chemical Property:

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Technology Process of PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

There total 2 articles about PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: aluminium oxide

: 10026-13-8,874483-75-7
phosphorus pentachloride

: 18460-53-2
PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

: 10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate

Guidance literature:: In neat (no solvent); exclusion of moisture; heating (523 K, 2 - 80 h, ratio PCl5:Al2O3 = 5:1), in a sealed tube; partial evapn. of POCl3;

Reference yield:

: 12588-13-5
SeCl₃⁽¹⁺⁾*AlCl₄^(1-)=(SeCl₃)(AlCl₄)

: phosphorus

: 18460-53-2
PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

: 7719-12-2,52843-90-0
phosphorus trichloride

Guidance literature:: In dichloromethane;
DOI:10.1039/c9sc03915e

Reference yield: 81.0%

: 18460-53-2
PCl₄⁽¹⁺⁾*AlCl₄^(1-)=PCl₄[AlCl₄]

: 56-37-1
N-benzyl-N,N,N-triethylammonium chloride

: 7681-11-0
potassium iodide

: 7719-12-2,52843-90-0
phosphorus trichloride

Guidance literature:: In neat (no solvent); argon atmosphere; KI and org. compd. addn. to PCl4AlCl4 (cooling), reaction vessel connecting to vac. line (2 mm Hg), mixt. heating to 80°C, liquefaction; volatiles collection (trap cooled with liq. nitrogen);