1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

Base Information

Chemical Name:1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate
CAS No.:167226-11-1
Molecular Formula:C₁₃H₁₅ClO₃
Molecular Weight:254.713
Hs Code.:

Synonyms:1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

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Chemical Property of 1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

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Technology Process of 1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

There total 1 articles about 1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 674-82-8,2130-41-8
4-methyleneoxetan-2-one

: 13524-04-4
2'-chloro-sec-phenethyl alcohol

: 74-88-4
methyl iodide

: 167226-11-1
1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

Guidance literature:: With triethylamine; N,N,N',N'-tetramethylguanidine; Yield given; Multistep reaction; 1.) benzene, RT, 12 h, 2.) benzene, RT, 2 days;
DOI:10.1006/bioo.1998.1106

Reference yield: 35.0%

: 167226-11-1
1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

: 1-(2-chlorophenyl)ethyl 3-hydroxy-2-methylbutyrate

Guidance literature:: With buffer Mopso; YKER-I; NADPH; In water; at 30 ℃;
DOI:10.1006/bioo.1998.1106

Reference yield:

: 167226-11-1
1-(2-chlorophenyl)ethyl 2-methyl-3-oxobutyrate

: (2R,3S)-3-Hydroxy-2-methyl-butyric acid (S)-1-(2-chloro-phenyl)-ethyl ester

: (2R,3S)-3-Hydroxy-2-methyl-butyric acid (R)-1-(2-chloro-phenyl)-ethyl ester

Guidance literature:: In water; at 30 ℃; for 18h; Yield given. Yields of byproduct given; NADPH, L-enzyme-1, 3-hydroxy-4-morpholinepropanesulfonate buffer, Glucose-6-phosphate, Glucose-6-phosphate dehydrogenase;
DOI:10.1016/0040-4039(94)02260-I