DYNORPHIN A (1-11) AMIDE

Base Information

• Chemical Name: DYNORPHIN A (1-11) AMIDE
• CAS No.: 79985-48-1
• Molecular Formula: C63H104 N22 O12
• Molecular Weight: 1361.66
• Mol file: 79985-48-1.mol

Synonyms:a-Neoendorphin (pig),7-L-arginine-8-L-isoleucine-8a-endo-L-arginine-10-L-lysinamide-; DynorphinA(1-11)-NH2

Chemical Property of DYNORPHIN A (1-11) AMIDE

Chemical Property:

• PSA: 583.27000
• LogP: 4.74770
• Storage Temp.: -15°C

Purity/Quality:

98% ^*data from raw suppliers

DYNORPHIN A (1-11) AMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DYNORPHIN A (1-11) AMIDE

There total 6 articles about DYNORPHIN A (1-11) AMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H30NO7Pol + N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Leu-OH (35661-60-0) + Fmoc-Pro-OH (71989-31-6) + N-Fmoc L-Phe (35661-40-6) + Fmoc-Ile-OH (71989-23-6,251316-98-0) + Fmoc-Tyr(tBu)-OH (71989-38-3,118488-18-9,204384-67-8) + Fmoc-Lys(tert-butoxycarbonyl) (71989-26-9) + Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine (187618-60-6) → Dynorphin A-(1-11) amide (79985-48-1)

Guidance literature:

C₂₉H₃₀NO₇Pol; With piperidine; In N,N-dimethyl-formamide; for 0.333333h; solid phase reaction;

Fmoc-Lys(tert-butoxycarbonyl); With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide; for 2h; solid phase reaction;

N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Leu-OH; Fmoc-Pro-OH; N-Fmoc L-Phe; Fmoc-Ile-OH; Fmoc-Tyr(tBu)-OH; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; Further stages;

DOI:10.1021/jm900715m

Reference yield:

1-(tert-butoxycarbonyl)-L-proline (15761-39-4,59433-50-0) + N-(tert-butyloxycarbonyl)-L-isoleucine (13139-16-7) + Nα-Boc-NG-tosyl-L-arginine (13836-37-8) + Nα-Boc-Nε-(2,4-dichlorobenzyloxycarbonyl)-L-lysine (42294-64-4) → Dynorphin A-(1-11) amide (79985-48-1)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jm00169a007

Reference yield:

1-(tert-butoxycarbonyl)-L-proline (15761-39-4,59433-50-0) + N-(tert-butyloxycarbonyl)-L-isoleucine (13139-16-7) + Nα-Boc-NG-tosyl-L-arginine (13836-37-8) + Nα-Boc-Nε-(2,4-dichlorobenzyloxycarbonyl)-L-lysine (42294-64-4) → Dynorphin A-(1-11) amide (79985-48-1)

Guidance literature:

Multistep reaction;

DOI:10.1021/jm00049a010

upstream raw materials:

1-(tert-butoxycarbonyl)-L-proline

N-(tert-butyloxycarbonyl)-L-isoleucine

N^α-Boc-N^G-tosyl-L-arginine

N^α-Boc-N^ε-(2,4-dichlorobenzyloxycarbonyl)-L-lysine

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