2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

Base Information

Chemical Name:2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate
CAS No.:918948-06-8
Molecular Formula:C₃₁H₂₇N₃O₇
Molecular Weight:553.571
Hs Code.:

Synonyms:2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

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Technology Process of 2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

There total 3 articles about 2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 918948-03-5
2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

: 918948-06-8
2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

Guidance literature:: With tetrahydrofuran; borane; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol062464t

Reference yield:

: 98-88-4
benzoyl chloride

: 918948-06-8
2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / cooling

2: 89 percent / borane/tetrahydrofuran complex; copper(II) trifluoromethanesulfonate / tetrahydrofuran / 20 °C

With tetrahydrofuran; dmap; borane; copper(II) bis(trifluoromethanesulfonate); triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol062464t

Reference yield:

: (2R,4aR,7R,8R,8aS)-7-Azido-2-naphthalen-2-yl-hexahydro-pyrano[3,2-d][1,3]dioxine-6,8-diol

: 918948-06-8
2-azido-3-O-benzoyl-2-deoxy-4-O-(2-naphthylmethyl)-β-D-glucopyranosyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / cooling

2: 89 percent / borane/tetrahydrofuran complex; copper(II) trifluoromethanesulfonate / tetrahydrofuran / 20 °C

With tetrahydrofuran; dmap; borane; copper(II) bis(trifluoromethanesulfonate); triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol062464t