2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Base Information

Chemical Name:2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate
CAS No.:918948-03-5
Molecular Formula:C₃₁H₂₅N₃O₇
Molecular Weight:551.555
Hs Code.:

Synonyms:2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

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Chemical Property of 2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

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Technology Process of 2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

There total 5 articles about 2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₁₈H₁₉N₃O₅

: 98-88-4
benzoyl chloride

: 918948-03-5
2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 92.0%

: 98-88-4
benzoyl chloride

: (2R,4aR,7R,8R,8aS)-7-Azido-2-naphthalen-2-yl-hexahydro-pyrano[3,2-d][1,3]dioxine-6,8-diol

: 918948-03-5
2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; cooling;
DOI:10.1021/ol062464t

Reference yield:

: 93-97-0
benzoic acid anhydride

: (2R,4aR,7R,8R,8aS)-7-Azido-2-naphthalen-2-yl-hexahydro-pyrano[3,2-d][1,3]dioxine-6,8-diol

: 918948-03-5
2-azido-3-O-benzoyl-2-deoxy-4,6-O-(2-naphthylmethylidene)-β-D-glucopyranosyl benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo101320r