N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Base Information

Chemical Name:N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide
CAS No.:1421703-96-9
Molecular Formula:C₃₈H₄₈N₆O₃
Molecular Weight:636.838
Hs Code.:

Synonyms:N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

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Chemical Property of N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

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Technology Process of N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

There total 3 articles about N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1421703-95-8
ethyl 2-(diphenylmethyleneamino)-7-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)heptanoate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1421703-96-9
N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: With isopropylmagnesium chloride; In tetrahydrofuran; at -20 - 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cmdc.201200350

Reference yield:

: 1353046-53-3
ethyl 2-(diphenylmethyleneamino)non-8-ynoate

: 1421703-96-9
N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate / dichloromethane; tert-butyl alcohol; water / 12 h / 20 °C

2: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -20 - 0 °C / Inert atmosphere

With isopropylmagnesium chloride; copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/cmdc.201200350

Reference yield:

: 1192358-22-7
N-(2-azidoethyl)-4-pentylbenzamide

: 1421703-96-9
N-(2-(4-(6-(diphenylmethyleneamino)-7-(methoxy-(methyl)amino)-7-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate / dichloromethane; tert-butyl alcohol; water / 12 h / 20 °C

2: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -20 - 0 °C / Inert atmosphere

With isopropylmagnesium chloride; copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/cmdc.201200350