pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate

Base Information

• Chemical Name: pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate
• CAS No.: 1214285-48-9
• Molecular Formula: C₄₄H₅₇N₅O₉
• Molecular Weight: 799.965

Synonyms:pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate

Chemical Property of pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate

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Technology Process of pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate

There total 1 articles about pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-(benzyloxycarbonyl)-4-hydroxypiperidine (95798-23-5) + pentyl 4-((2S)-5-tert-butoxy-2-([(4-hydroxy-6-phenylpyridin-2-yl)carbonyl]amino)-5-oxopentanoyl)piperazine-1-carboxylate (1214284-55-5) → pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate (1214285-48-9)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 5 - 20 ℃;

DOI:10.1021/jm901518t

Reference yield: 82.0%

pentyl 4-[(2S)-2-(([4-((1-[(benzyloxy)carbonyl]piperidin-4-yl)-oxy)-6-phenylpyridin-2-yl]carbonyl)amino)-5-tert-butoxy-5-oxopentanoyl]piperazine-1-carboxylate (1214285-48-9) → pentyl 4-[(2S)-5-tert-butoxy-5-oxo-2-(([6-phenyl-4-(piperidin-4-yloxy)pyridin-2-yl]carbonyl)amino)pentanoyl]piperazine-1-carboxylate (1214285-52-5)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; for 16h; under 2068.65 Torr;

DOI:10.1021/jm901518t

upstream raw materials:

1-(benzyloxycarbonyl)-4-hydroxypiperidine

pentyl 4-((2S)-5-tert-butoxy-2-([(4-hydroxy-6-phenylpyridin-2-yl)carbonyl]amino)-5-oxopentanoyl)piperazine-1-carboxylate

Downstream raw materials:

pentyl 4-[(2S)-5-tert-butoxy-5-oxo-2-(([6-phenyl-4-(piperidin-4-yloxy)pyridin-2-yl]carbonyl)amino)pentanoyl]piperazine-1-carboxylate

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