3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

Base Information

Chemical Name:3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE
CAS No.:1308870-46-3
Molecular Formula:C₃₀H₂₉N₃
Molecular Weight:431.58
Hs Code.:

Synonyms:3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

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Chemical Property of 3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

Chemical Property:

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Technology Process of 3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

There total 12 articles about 3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1308870-44-1
C₂₄H₂₀BrN₃

: 89490-05-1,21190-87-4
cyclohex-1-enylboronic acid

: 1308870-46-3
3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

Guidance literature:: With potassium acetate; bis(tri-tert-butylphasphine)palladium dichloride; In water; acetonitrile; at 120 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 38940-62-4
3-acetyl-5-bromopyridine

: 1308870-46-3
3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol; sodium tetrahydroborate / 0.5 h / 20 °C

2.1: thionyl chloride / dichloromethane / 4 h / 20 °C

3.1: lithium bromide / 1,4-dioxane / 120 °C / Sealed vessel

4.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0 °C / Inert atmosphere

4.2: 1.67 h / 20 °C / Cooling with ice

5.1: 1-methyl-pyrrolidin-2-one / 1.17 h / 200 °C

6.1: trifluoroacetic acid / 1 h / 90 °C

7.1: potassium acetate / bis(tri-tert-butylphasphine)palladium dichloride / acetonitrile; water / 0.17 h / 120 °C / Microwave irradiation

With sodium tetrahydroborate; thionyl chloride; ethanol; potassium acetate; potassium hexamethylsilazane; trifluoroacetic acid; lithium bromide; bis(tri-tert-butylphasphine)palladium dichloride; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 283608-66-2
1-(5-bromo-pyridin-3-yl)-ethanol

: 1308870-46-3
3-(2-(5-(cyclohexenyl)pyridin-3-yl)prop-1-enyl)-6-o-tolylquinolin-2-amiE

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / dichloromethane / 4 h / 20 °C

2.1: lithium bromide / 1,4-dioxane / 120 °C / Sealed vessel

3.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0 °C / Inert atmosphere

3.2: 1.67 h / 20 °C / Cooling with ice

4.1: 1-methyl-pyrrolidin-2-one / 1.17 h / 200 °C

5.1: trifluoroacetic acid / 1 h / 90 °C

6.1: potassium acetate / bis(tri-tert-butylphasphine)palladium dichloride / acetonitrile; water / 0.17 h / 120 °C / Microwave irradiation

With thionyl chloride; potassium acetate; potassium hexamethylsilazane; trifluoroacetic acid; lithium bromide; bis(tri-tert-butylphasphine)palladium dichloride; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; dichloromethane; water; toluene; acetonitrile;