dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

Base Information

Chemical Name:dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester
CAS No.:1070800-64-4
Molecular Formula:C₃₆H₄₅Cl₃O₈S₂
Molecular Weight:776.239
Hs Code.:

dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

Synonyms:dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

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Chemical Property of dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

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Technology Process of dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

There total 1 articles about dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1070800-59-7
(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-en-1-ol

: 74-88-4
methyl iodide

: 1070800-64-4
dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

Guidance literature:: (1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-en-1-ol; With water; sodium hydride; In tetrahydrofuran; at 23 ℃; for 0.166667h; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; at 23 ℃; for 0.333333h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 23 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol8018727

Reference yield:

: 1070800-64-4
dithiocarbonic acid {(1R,2S)-1-(3-benzyloxymethoxy-2-vinylphenyl)-2-[(1S,2S)-1-methoxy-2-((2S,3R)-3-methyl-1,4-dioxaspiro[4.4]non-2-yl)-2-(2,2,2-trichloroethoxymethoxy)ethyl]but-3-enyl} ester methyl ester

: 1070800-66-6
C₃₄H₄₃Cl₃O₇

Guidance literature:: With triethyl borane; oxygen; tri-n-butyl-tin hydride; In hexane; toluene; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol8018727