Technology Process of (2S,4S)-2-((benzyloxy)methyl)-1,3-dioxolane-4-carboxylic acid
There total 6 articles about (2S,4S)-2-((benzyloxy)methyl)-1,3-dioxolane-4-carboxylic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hypochlorite; ruthenium(III) trichloride hydrate; sodium hydroxide;
In
water;
at 20 - 35 ℃;
for 15h;
pH=8;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: TsOH / acetonitrile
2: 1.) 30percent aq. H2O2, K2CO3, 2.) RuCl3 hydrate, NaOCl, BnEt3NCl / 2.) DCE, MeCN, H2O
With
ruthenium trichloride; sodium hypochlorite; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; potassium carbonate; toluene-4-sulfonic acid;
In
acetonitrile;
DOI:10.1016/S0957-4166(00)80092-0
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / N,N-dimethyl-formamide / 16 h / 0 - 20 °C
2: toluene-4-sulfonic acid / acetonitrile / 1 h / 90 °C
3: dihydrogen peroxide; potassium carbonate / water / 24 h / 0 °C
4: sodium hypochlorite; ruthenium(III) trichloride hydrate; sodium hydroxide / water / 15 h / 20 - 35 °C / pH 8
With
sodium hypochlorite; ruthenium(III) trichloride hydrate; dihydrogen peroxide; potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide;
In
water; N,N-dimethyl-formamide; acetonitrile;
