but-2-enyl cinnamyl ether

Base Information

• Chemical Name: but-2-enyl cinnamyl ether
• CAS No.: 100611-67-4
• Molecular Formula: C₁₃H₁₆O
• Molecular Weight: 188.269
• Mol file: 100611-67-4.mol

Synonyms:but-2-enyl cinnamyl ether

Chemical Property of but-2-enyl cinnamyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of but-2-enyl cinnamyl ether

There total 1 articles about but-2-enyl cinnamyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Phenylpropenol (104-54-1) + buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → but-2-enyl cinnamyl ether (100611-67-4) + C13H16O

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,2-bis((diphenylphosphino)methyl)benzene; In toluene; at -15 - 80 ℃; Reagent/catalyst; chemoselective reaction; Inert atmosphere; Glovebox; Schlenk technique;

DOI:10.1002/adsc.201500721

Reference yield: 49.4%

bis(ethylene)rhodium acetylacetonate + but-2-enyl cinnamyl ether (100611-67-4) → Rh(but-2-enyl cinnamyl ether)(pentane-2,4-dionate) (67407-50-5)

Guidance literature:

In pentane; byproducts: ethylene; addn. of excess diene to Rh-complex (room temp., stirring for 12 h); filtration of first crop of product, concn. of filtrate, trituration with pentane, recrystn. (pentane); elem. anal.;

DOI:10.1039/DT9780000333

Reference yield: 49.0%

but-2-enyl cinnamyl ether (100611-67-4) + 1-methyl-4-nitrobenzene (99-99-0) → C20H25NO

Guidance literature:

With Triethoxysilane; C₂₅H₂₂FeNPS; In tetrahydrofuran; at 40 ℃; for 24h;

DOI:10.1021/acscatal.9b03604

upstream raw materials:

3-Phenylpropenol

buta-1,3-diene

Downstream raw materials:

Rh(but-2-enyl cinnamyl ether)(pentane-2,4-dionate)