2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid

Base Information

• Chemical Name: 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid
• CAS No.: 1333325-53-3
• Molecular Formula: C₃₂H₂₈O₈
• Molecular Weight: 540.57

Synonyms:2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid

Chemical Property of 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid

Chemical Property:

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Technology Process of 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid

There total 3 articles about 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-benzyl 3-methyl 2,6-bis(benzyloxy)-4-(2-methoxy-2-oxoethyl)isophthalate (1333325-37-3) → 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid (1333325-53-3)

Guidance literature:

With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

DOI:10.1021/ol202265g

Reference yield:

dimethyl 4-carboxy-3,5-dihydroxyhomophthalate (6121-79-5) → 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid (1333325-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 19 h / Reflux

2: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h / 0 - 20 °C

With lithium hydroxide monohydrate; water; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/ol202265g

Reference yield:

benzyl bromide (100-39-0) → 2-(3,5-bis(benzyloxy)-4-(benzyloxycarbonyl)-2-(methoxycarbonyl)phenyl)acetic acid (1333325-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 19 h / Reflux

2: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h / 0 - 20 °C

With lithium hydroxide monohydrate; water; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/ol202265g

upstream raw materials:

1-benzyl 3-methyl 2,6-bis(benzyloxy)-4-(2-methoxy-2-oxoethyl)isophthalate

dimethyl 4-carboxy-3,5-dihydroxyhomophthalate

benzyl bromide

Downstream raw materials:

2-propenyl (2S,3S,3'aS,4S,5'R)-4-[2-[(1,1-dimethylethyl)diphenylsilyloxy]ethyl]-3',3'a,4,5,5',6'-hexahydro-3-methyl-5'-pentyl-8'-(2-propenyloxy)-spiro[furan-2(3H),2'-[2H]pyrano[2,3,4-de][1]benzopyran]-9'-carboxylate

C₃₉H₅₀O₇Si

(3R)-benzyl 6,8-bis(benzyloxy)-1-oxo-3-pentylisochroman-7-carboxylate

(3R)-benzyl 6,8-bis(benzyloxy)-1-hydroxy-3-pentylisochroman-7-carboxylate

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