N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Base Information

• Chemical Name: N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide
• CAS No.: 98319-30-3
• Molecular Formula: C₂₁H₁₇N₅O₄
• Molecular Weight: 403.397
• Mol file: 98319-30-3.mol

Synonyms:N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Chemical Property of N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Chemical Property:

Purity/Quality:

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Technology Process of N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

There total 1 articles about N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

pyridine-2,6-dicarbohydrazide (5112-36-7) + salicylaldehyde (90-02-8) → N2,N6-bis(salicylidene)pyridine-2,6-dicarbohydrazide (98319-30-3)

Guidance literature:

With zinc(II) perchlorate; In ethanol; Reflux;

DOI:10.1039/c6dt00612d

Reference yield: 94.0%

N2,N6-bis(salicylidene)pyridine-2,6-dicarbohydrazide (98319-30-3) + copper(II) acetate monohydrate (6046-93-1) → 2H(1+)*2Cu(2+)*C21H15N5O4(2-)*4CH3CO2(1-) = H2[Cu2(C21H15N5O4)(O2CCH3)4]

Guidance literature:

In dimethyl sulfoxide; addn. of solid Cu(OAc)2*H2O to the ligand in DMSO, stirring (room temp.,1 h), addn. of further Cu(OAc)2*H2O in DMSO, heating to 80°C for 5 h; filtration, washing (EtOH), drying (vac.); elem. anal.;

DOI:10.1039/a603850f

Reference yield: 92.0%

N2,N6-bis(salicylidene)pyridine-2,6-dicarbohydrazide (98319-30-3) + uranyl(VI) acetate dihydrate → UO2(OC6H4CHNNCOC5H3NCONHNHCHC6H4O)(CH3CH2OH)2

Guidance literature:

In pyridine; ethanol; addn. of an ethanolic soln. of uranyl acetate dihydrate to a soln. of ligand in a mixt. of abs. ethanol/pyridine, stirring resulting mixt. (containig an orange product) at room temp. for 18 h; filtration, washing several times with abs. ethanol, drying in vacuo, elem. anal.;

DOI:10.1016/S0020-1693(00)81346-8

upstream raw materials:

pyridine-2,6-dicarbohydrazide

salicylaldehyde