N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Base Information

Chemical Name:N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide
CAS No.:98319-30-3
Molecular Formula:C₂₁H₁₇N₅O₄
Molecular Weight:403.397
Hs Code.:

N<SUP>2</SUP>,N<SUP>6</SUP>-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Synonyms:N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

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Chemical Property of N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

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Technology Process of N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

There total 1 articles about N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5112-36-7
pyridine-2,6-dicarbohydrazide

: 90-02-8
salicylaldehyde

: 98319-30-3
N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

Guidance literature:: With zinc(II) perchlorate; In ethanol; Reflux;
DOI:10.1039/c6dt00612d

Reference yield: 94.0%

: 98319-30-3
N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

: 6046-93-1
copper(II) acetate monohydrate

: 2H⁽¹⁺⁾*2Cu⁽²⁺⁾*C₂₁H₁₅N₅O₄^(2-)*4CH₃CO₂^(1-) = H₂[Cu₂(C₂₁H₁₅N₅O₄)(O₂CCH₃)4]

Guidance literature:: In dimethyl sulfoxide; addn. of solid Cu(OAc)2*H2O to the ligand in DMSO, stirring (room temp.,1 h), addn. of further Cu(OAc)2*H2O in DMSO, heating to 80°C for 5 h; filtration, washing (EtOH), drying (vac.); elem. anal.;
DOI:10.1039/a603850f

Reference yield: 92.0%

: 98319-30-3
N²,N⁶-bis(salicylidene)pyridine-2,6-dicarbohydrazide

: uranyl(VI) acetate dihydrate

: UO₂(OC₆H₄CHNNCOC₅H₃NCONHNHCHC₆H₄O)(CH₃CH₂OH)2

Guidance literature:: In pyridine; ethanol; addn. of an ethanolic soln. of uranyl acetate dihydrate to a soln. of ligand in a mixt. of abs. ethanol/pyridine, stirring resulting mixt. (containig an orange product) at room temp. for 18 h; filtration, washing several times with abs. ethanol, drying in vacuo, elem. anal.;
DOI:10.1016/S0020-1693(00)81346-8