10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

Base Information

Chemical Name:10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol
CAS No.:1356140-46-9
Molecular Formula:C₄₃H₈₀O₃
Molecular Weight:645.106
Hs Code.:

Synonyms:10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

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Chemical Property of 10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

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Technology Process of 10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

There total 7 articles about 10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1187663-05-3
diethyl 5-[3-(benzyloxy)propyl]nonanedioate

: 626-88-0
1-bromo-5-methylpentane

: 1356140-46-9
10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

Guidance literature:: 1-bromo-5-methylpentane; With iodine; magnesium; In diethyl ether; for 2h; Inert atmosphere; Reflux;

diethyl 5-[3-(benzyloxy)propyl]nonanedioate; In diethyl ether; for 5h; Inert atmosphere; Reflux;
DOI:10.1002/asia.201100480

Reference yield:

: 4541-14-4
4-benzyloxy-butan-1-ol

: 1356140-46-9
10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

Guidance literature:: Multi-step reaction with 7 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 6 h / Cooling with ice

5.1: Jones reagent / acetone

6.1: sulfuric acid / 12 h / Reflux

6.2: 6 h / 20 °C / 760.05 Torr

7.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

7.2: 5 h / Inert atmosphere; Reflux

With Jones reagent; ammonium cerium (IV) nitrate; sulfuric acid; iodine; magnesium; In diethyl ether; water; acetone; acetonitrile; 1.1: Jones oxidation / 5.1: Jones oxidation;
DOI:10.1002/asia.201100480

Reference yield:

: 1187663-04-2
C₁₉H₃₂O₄

: 1356140-46-9
10-[3-(benzyloxy)propyl]-2,18-dimethyl-6,14-bis(4-methylpentyl)nonadecane-6,14-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

2.2: 6 h / 20 °C / 760.05 Torr

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

With Jones reagent; sulfuric acid; iodine; magnesium; In diethyl ether; acetone; 1.1: Jones oxidation;
DOI:10.1002/asia.201100480