N-(triphenylphosphinegold) acetamide

Base Information

Chemical Name:N-(triphenylphosphinegold) acetamide
CAS No.:117199-33-4
Molecular Formula:C₂₀H₁₉AuNOP
Molecular Weight:517.317
Hs Code.:

Synonyms:N-(triphenylphosphinegold) acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(triphenylphosphinegold) acetamide

Chemical Property:

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Technology Process of N-(triphenylphosphinegold) acetamide

There total 1 articles about N-(triphenylphosphinegold) acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 60-35-5
acetamide

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 7646-69-7
sodium hydride

: 117199-33-4
N-(triphenylphosphinegold) acetamide

Guidance literature:: In tetrahydrofuran; a suspn. of 0.24 g of acetamide and 0.1 g of NaH in THF is treated with 1 g of Ph3PAuCl; the mixt. is stirred until the initial gold salt has disappeared (1 h); reaction mixt. treated with water; soln. dried (K2CO3), solvent removed; residue dissolved in methyl ethyl ketone, Au complex pptd. by addn. of ether/petroleum ether (4:1); ppt. filtered off and dried under vac. over wax and P2O5 (36°C, 4 h); elem. anal.;

Reference yield:

: 117199-33-4
N-(triphenylphosphinegold) acetamide

: 7440-57-5,457905-15-6
gold

Guidance literature:: In not given; decompn. in soln.;

Reference yield:

: 117199-33-4
N-(triphenylphosphinegold) acetamide

: 14243-64-2
(triphenylphosphine)gold(I) chloride

Guidance literature:: With HCl; In chloroform; water; 0.1 N HCl added to a soln. of the gold complex in CHCl3; mixt. stirred for 30 min; organic layer sepd. off, washed with water, and dried with K2CO3; CHCl3 removed at reduced pressure;