(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

Base Information

Chemical Name:(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside
CAS No.:1246763-92-7
Molecular Formula:C₂₂H₂₃N₅O₆
Molecular Weight:453.455
Hs Code.:

Synonyms:(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

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Chemical Property of (N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

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Technology Process of (N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

There total 7 articles about (N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1246763-86-9
4,6-di-O-acetyl-1,2,3-trideoxy-1-(phenylsulfinyl)-L-erythro-hexopyranose

: 4005-49-6
N-benzoyladenine

: 60873-27-0
C₁₀H₁₄O₅

: 1246763-89-2
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-β-L-erythro-hexopyranoside

: 1246763-92-7
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

Guidance literature:: 4,6-di-O-acetyl-1,2,3-trideoxy-1-(phenylsulfinyl)-L-erythro-hexopyranose; N-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 60 ℃; for 0.5h; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 20 - 60 ℃; for 48.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo100691y

Reference yield: 65.0%

: 1,4,6-tri-O-acetyl-2,3-dideoxy-L-erythro-hexopyranose

: 4005-49-6
N-benzoyladenine

: 60873-27-0
C₁₀H₁₄O₅

: 1246763-89-2
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-β-L-erythro-hexopyranoside

: 1246763-92-7
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

Guidance literature:: N-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 1h; Inert atmosphere; Reflux;

1,4,6-tri-O-acetyl-2,3-dideoxy-L-erythro-hexopyranose; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 30 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo100691y

Reference yield: 47.0%

: 4,6-di-O-acetyl-2,3-dideoxy-α-L-erythro-hexopyranosyl iodide

: 4005-49-6
N-benzoyladenine

: 60873-27-0
C₁₀H₁₄O₅

: 1246763-89-2
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-β-L-erythro-hexopyranoside

: 1246763-92-7
(N6-benzoyladenin-9-yl) 4,6-di-O-acetyl-1,2,3-trideoxy-α-L-erythro-hexopyranoside

Guidance literature:: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo100691y