3-(benzenesulfonyl)-4-phenoxyfuroxan

Base Information

• Chemical Name: 3-(benzenesulfonyl)-4-phenoxyfuroxan
• CAS No.: 1237752-72-5
• Molecular Formula: C₁₄H₁₀N₂O₅S
• Molecular Weight: 318.31
• Mol file: 1237752-72-5.mol

Synonyms:3-(benzenesulfonyl)-4-phenoxyfuroxan

Chemical Property of 3-(benzenesulfonyl)-4-phenoxyfuroxan

Chemical Property:

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Technology Process of 3-(benzenesulfonyl)-4-phenoxyfuroxan

There total 1 articles about 3-(benzenesulfonyl)-4-phenoxyfuroxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (66074-00-8) + phenol (108-95-2,27073-41-2) → 3-(benzenesulfonyl)-4-phenoxyfuroxan (1237752-72-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h; regioselective reaction;

DOI:10.1021/jm100066y

Reference yield: 75.0%

3-(benzenesulfonyl)-4-phenoxyfuroxan (1237752-72-5) + 4-Phenylbutyric acid (1821-12-1) → 4-phenoxy-3-(3-phenylpropyl)furoxan

Guidance literature:

With dipotassium peroxodisulfate; silver nitrate; In water; acetonitrile; at 70 ℃; for 30h; regioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.0c00062

upstream raw materials:

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

phenol