benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

Base Information

Chemical Name:benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate
CAS No.:1439909-59-7
Molecular Formula:C₂₆H₃₀N₆O₃
Molecular Weight:474.563
Hs Code.:

Synonyms:benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

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Chemical Property of benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

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Technology Process of benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

There total 4 articles about benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 227449-48-1
2-((1H-benzo[d][1,2,3]triazol-1-yl)oxy)-4-(m-tolylamino)pyrimidin-5-carboxamide

: 1439908-64-1
benzyl 1-(1-aminopropyl)cyclopropylcarbamate

: 1439909-59-7
benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 60 ℃; for 3h;

Reference yield:

: 84677-06-5
(benzyloxycarbonylamino)cyclopropanecarboxylic acid

: 1439909-59-7
benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: tetrahydrofuran / 2 h / 20 °C

3.1: ammonium chloride; titanium(IV) isopropylate; triethylamine / ethanol / 15 h / 20 °C

3.2: 48 h

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h / 60 °C

With titanium(IV) isopropylate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 851726-81-3
benzyl {1-[methoxy(methyl)carbamoyl]cyclopropyl}carbamate

: 1439909-59-7
benzyl 1-(1-(5-carbamoyl-4-(m-tolylamino)pyrimidin-2-ylamino)propyl)cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 2 h / 20 °C

2.1: ammonium chloride; titanium(IV) isopropylate; triethylamine / ethanol / 15 h / 20 °C

2.2: 48 h

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h / 60 °C

With titanium(IV) isopropylate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetonitrile;