((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

Base Information

Chemical Name:((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride
CAS No.:1185287-64-2
Molecular Formula:C₁₅H₂₂N₂O₃*ClH
Molecular Weight:314.812
Hs Code.:

Synonyms:((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

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Chemical Property of ((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

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Technology Process of ((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

There total 3 articles about ((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1185287-63-1
((S)-2-tert-butoxycarbonylamino-3,3-dimethylbutyrylamino)acetic acid benzyl ester

: 1185287-64-2
((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 18 - 25 ℃; for 4h; Inert atmosphere;

Reference yield:

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 1185287-64-2
((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 18 - 25 °C / Inert atmosphere

1.2: 18 h / 18 - 25 °C

2.1: hydrogenchloride / 1,4-dioxane / 4 h / 18 - 25 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 62965-35-9
N-tert-butyloxycarbonyl-L-tert-leucine

: 1185287-64-2
((S)-2-amino-3,3-dimethyl butyrylamino)acetic acid benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 18 - 25 °C / Inert atmosphere

1.2: 18 h / 18 - 25 °C

2.1: hydrogenchloride / 1,4-dioxane / 4 h / 18 - 25 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;