6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Base Information

Chemical Name:6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide
CAS No.:120344-68-5
Molecular Formula:Br*C₂₅H₂₀ClN₂O₂S₂
Molecular Weight:559.935
Hs Code.:

Synonyms:6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

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Chemical Property of 6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

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Technology Process of 6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

There total 3 articles about 6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 23149-96-4
4-(p-Methoxybenzylidene)amino-3-phenylthiazoline-2(3H)-thione

: 536-38-9
4-chlorobenzoylmethyl bromide

: 120344-68-5
6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Guidance literature:: With acetic acid; In isopropyl alcohol; 1.) reflux, 5 min, 2.) room temp., 30 min;
DOI:10.1055/s-1988-27691

Reference yield:

: 5316-81-4
3-amino-4-phenylthiazoline-2(3H)-thione

: 120344-68-5
6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / NaOAc / aq. ethanol / 0.5 h / Heating

2: 75 percent / HOAc / propan-2-ol / 1.) reflux, 5 min, 2.) room temp., 30 min

With sodium acetate; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1055/s-1988-27691

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 120344-68-5
6-(4-Chloro-benzoyl)-5-(4-methoxy-phenyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / NaOAc / aq. ethanol / 0.5 h / Heating

2: 75 percent / HOAc / propan-2-ol / 1.) reflux, 5 min, 2.) room temp., 30 min

With sodium acetate; acetic acid; In ethanol; isopropyl alcohol;
DOI:10.1055/s-1988-27691